Electron diffraction facility

More Information

¾ÅÉ«ÊÓÆµ the electron diffraction facility

Our electron diffraction facility enables single-crystal structure analysis of crystallites too small for single-crystal X-ray diffraction (SCXRD) experiments.

We can obtain data from grains well below 1 micrometre and determine their crystal structure in an analogous way as is used in SCXRD.

Measurements are conducted using the continuous rotation method, allowing rapid data collections.

Compounds across a wide range of research areas can be used, including, but not limited to: 

  • small organics
  • natural products
  • metalorganic complexes porous materials
  • inorganics

Data collections can be performed routinely from 100 Kelvin (K) to room temperature (rt). Additional elemental analysis of the crystals of interest is available using energy-dispersive X-ray spectroscopy (EDS). 

Our specialists have more than 20 plus years’ experience in materials characterisation, material science and electron microscopy. 

Technical specification

Rigaku XtaLAB Synergy-ED

  • LaB6 (Lanthanum Hexaboride) electron gun up to 200 kilovolt (kV)
  • high-speed, high-sensitivity photon-counting Rigaku HyPix-ED hybrid pixel array detector
  • JEOL JED-2200 energy-dispersive spectrometer

 

Holders

  • JEOL standard transmission electron microscope (TEM) holder with high-tilt retainer - rt experiments
  • Gatan Elsa cryogenic holder - rt to 100 K experiments
  • Hummingbird in situ gas-cell and heating holder  

 

Contact us

For more information, please contact us using the email addresses below

Professor Simon Coles

School of Chemistry and Chemical Engineering, ¾ÅÉ«ÊÓÆµ, Highfield Campus, ¾ÅÉ«ÊÓÆµ, SO17 1BJ 

Dr Mark Light

Dr Daniel N Rainer

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